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有读书笔记有附件Synthesis and properties of hot pressed B4C–TiB2 ceramic composite

1 浮标 添加于 2010-10-29 15:07 | 2325 次阅读 | 0 个评论
  •  作 者

    Yue XY, Zhao SM, Lü P, Chang Q, Ru HQ
  •  摘 要

    In order to improve the fracture toughness of B4C ceramics, B4C–TiB2 composite was prepared by hot pressing using B4C, C and TiCl4 as starting materials. The precursor powders of Ti(OH)4 and B4C were obtained using co-precipitation method. The phases, mechanical properties and microstructures of the B4C–TiB2 composite were investigated. The results showed that Ti(OH)4 almost converted into rutile TiO2 phase at 573 K for 1 h. The B4C–TiB2 composite with 43 mass% TiB2 showed the optimized mechanical properties. The optimum relative density, hardness, flexural strength and fracture toughness were 99.8%, 23.6 GPa, 506 MPa and 9.4 MPa m1/2, respectively. A number of twins and nanosecond-phase particles were observed in the B4C–TiB2 composite.
  •  详细资料

    • 文献种类: Journal Article
    • 期刊名称: Materials Science and Engineering: A
    • 期刊缩写: Materials Science and Engineering: A
    • 期卷页: 2010  527 27-28 7215-7219
    • ISBN: 0921-5093
  • 学科领域 工程技术 » 材料科学

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  •  附 件

    PDF附件Synthesis and properties of hot pressed B4C–TiB2 ceramic composite 
  •  浮标 的文献笔记  订阅

    反应热压烧结制备B4C-TiB2复相陶瓷:以沉淀TiO2为前驱体

    用TiCl4水解产生的TiO2,酚醛树脂裂解产生的C及商业B4C粉为原料,原位反应烧结制备了B4C-TiB2复相陶瓷。

    使用这种方法,原位合成的TiB2颗粒尺寸细小。

    B4C-43wt%TiB2复相陶瓷的三点抗弯强度只有506MPa,而断裂韧性却高达MPam1/2。

    内晶型结构+孪晶=高断裂韧性?  强度为什么没有提高?

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